Carbon Disulfide → 5-Hydroxypentyl isothiocyanate
반응식
[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH2:7].[C:8](=S)=[S:9].C(N(CC)CC)C.C(Cl)(=O)OCC>C(Cl)(Cl)Cl>[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][N:7]=[C:8]=[S:9]참가 물질
6
실험 절차
The synthesis method of Example 45-(1) was applied. 5-Hydroxypentylamine (6.00 g), carbon disulfide (40 ml), triethylamine (8.3 ml), ethyl chlorocarbonate (5.4 ml), triethylamine (8.3 ml) and chloroform (20 ml) were used as reagents. After the reaction, a yellow liquid was quantitatively obtained.
후처리
- customThe synthesis method of Example 45-(1)
- customAfter the reaction
- customa yellow liquid was quantitatively obtained
출처 및 근거
- ORD 기록
- ord-8df58fab982b4bcdb01a58c3cde4623e
- 출처 데이터셋
- uspto-grants-1998_05
- 특허 번호
- US05750545
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