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Toluene → HCID 136005564, 화합물

HRID 1350428
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HRID 1350428 반응식
[C:1]1([CH2:11][CH2:12][C@H:13]2[CH2:18][NH:17][CH2:16][CH2:15][NH:14]2)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[CH3:19][C:20]1[S:29][C:28]2[NH:27][C:26]3[CH:30]=[CH:31][CH:32]=[CH:33][C:25]=3[N:24]=[C:23](N)[C:22]=2[CH:21]=1.C1(C)C=CC=CC=1.C(N(C(C)C)C(C)C)C>C(OCC)(=O)C.O.C(O)(=O)C.CS(C)=O>[CH3:19][C:20]1[S:29][C:28]2[NH:27][C:26]3[CH:30]=[CH:31][CH:32]=[CH:33][C:25]=3[N:24]=[C:23]([N:17]3[CH2:16][CH2:15][NH:14][C@@H:13]([CH2:12][CH2:11][C:1]4[C:10]5[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=5)[CH:4]=[CH:3][CH:2]=4)[CH2:18]3)[C:22]=2[CH:21]=1
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참가 물질

9

반응물 4

HCID 1140TolueneHCID 81531DiisopropylethylamineHCID 58860672HCID 58860672, 화합물HCID 135446208Olanzamine

생성물 1

HCID 136005564HCID 136005564, 화합물수율 5%

시약·촉매·용매 4

HCID 176Acetic Acid용매
HCID 679
Dimethyl Sulfoxide
용매
HCID 962Water용매
HCID 8857Ethyl Acetate용매

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온도
105 °C

실험 절차

Combine (S)-2-(2-naphthalen-1-yl-ethyl)-piperazine (686 mg, 2.85 mmol), 2-methyl-4H-3-thia-4,9-diaza-benzo[f]azulen-10-ylamine (654 mg, 2.85 mmol), toluene (5.7 mL), DMSO (1.4 mL) and glacial acetic acid (0.5 mL). Add N-ethyldiisopropylamine (2.0 mL). Heat at 105° C. After 48 h, cool to ambient temperature and dilute with ethyl acetate and water. Extract with ethyl acetate. Wash the extracts with water and brine, dry over sodium sulfate, filter and concentrate the filtrate. Purify by silica gel chromatography using 2N ammonia in methanol-methylene chloride (0.5%–5%) as the eluent to give 183 mg. Purify again by radial silica gel chromatography using a 2 mm plate and 2N ammonia in methanol-methylene chloride (1%–2%) as the eluent to give 60 mg (5%) of the title compound: mass spectrum (ion spray): m/z=453 (M+1), 451 (M−1). Analysis calculated for C28H28N4S.0.2H2O: C, 73.71; H, 6.27; N, 12.28. Found: C, 73.37; H, 6.19; N, 12.00.

후처리

  1. temperaturecool to ambient temperature
  2. extractionExtract with ethyl acetate
  3. washWash the extracts with water and brine
  4. dry with materialdry over sodium sulfate
  5. filtrationfilter
  6. concentrationconcentrate the filtrate
  7. customPurify by silica gel chromatography
  8. customto give 183 mg
  9. customPurify again by radial silica gel chromatography

출처 및 근거

ORD 기록
ord-cfca0f2850d64d90851acc099a161228
출처 데이터셋
uspto-grants-2007_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07214673B2

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