Allyl chloride → HCID 22608987, 화합물

HRID 1380148노트

반응식

HRID 1380148 반응식
[Na].[C:2]([NH:5][C:6]#[N:7])(=[O:4])[CH3:3].[CH2:8](Cl)[CH:9]=[CH2:10]>S1(CCCC1)(=O)=O>[C:6]([N:5]([CH2:10][CH:9]=[CH2:8])[C:2](=[O:4])[CH3:3])#[N:7]

참가 물질

5

반응물 3

HCID 7850Allyl chlorideHCID 151267N-AcetylcyanamideHCID 5360545Sodium

생성물 1

HCID 22608987HCID 22608987, 화합물

시약·촉매·용매 1

HCID 31347Sulfolane용매

실험 절차

159.1 g (1.5 mols) of the sodium salt of acetylcyanamide and 137.8 g (1.5 mols+20% excess) of allyl chloride are reacted in 400 ml of sulfolane for 9 hours and 45 minutes at 70°-127° C. analogously to Example 1, and the mixture is worked up in accordance with Example 1. This gives 121.7 g (65.4% of theory) of a colourless distillate, boiling at 98° C./43 mbar.

출처 및 근거

ORD 기록
ord-07c999ba208745f099eef1a0ee27c832
출처 데이터셋
uspto-grants-1986_04
특허 번호
US04579933

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