1-(2-Methoxyethyl)-4-phenylimidazolidine-2-thione → Levamisole

HRID 1389552노트

반응식

HRID 1389552 반응식
CO[CH2:3][CH2:4][N:5]1[CH2:9][CH:8]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[NH:7][C:6]1=[S:16]>Cl.O>[CH2:4]1[N:5]2[C:6](=[N:7][C@@H:8]([C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=3)[CH2:9]2)[S:16][CH2:3]1

참가 물질

4

반응물 1

HCID 128034371-(2-Methoxyethyl)-4-phenylimidazolidine-2-thione

생성물 1

HCID 26879Levamisole

시약·촉매·용매 2

HCID 313Hydrochloric Acid용매HCID 962Water용매

실험 절차

The 1-2(methoxyethyl)-4-phenylimidazolidin-2-thione product of Example VII in the amount of 0.78 g is suspended in 50 ml concentrated aqueous hydrochloric acid and maintained with stirring at 70°-75° C. for four hours. The solution is then cooled at room temperature and diluted with 50 ml water.

후처리

  1. temperaturemaintained

출처 및 근거

ORD 기록
ord-aed09b4c53204ea7a74426f7309b1b0b
출처 데이터셋
uspto-grants-1981_01
특허 번호
US04245102

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