Methyl Methacrylate → Methyl Methacrylate

HRID 1447554

반응식

HRID 1447554 반응식
[C:1]([O:6][CH2:7][CH2:8][N:9]([CH2:12][CH3:13])[CH2:10][CH3:11])(=[O:5])[C:2]([CH3:4])=[CH2:3].C(OC)(=O)C(C)=C.CCCCCCCC/C=C\CCCCCCCCOCCO.C(OCCOC(=O)C=C)(=O)C=C.S(OOS([O-])(=O)=O)([O-])(=O)=O.[K+].[K+].S(=O)(O)[O-].[Na+]>O>[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:1]([O:6][CH2:7][CH2:8][N:9]([CH2:12][CH3:13])[CH2:10][CH3:11])(=[O:5])[CH:2]=[CH2:3]

참가 물질

9

반응물 6

HCID 6658Methyl MethacrylateHCID 24412Potassium PersulfateHCID 61012Diethylaminoethyl MethacrylateHCID 75282Ethylene glycol diacrylateHCID 5364713EmulphorHCID 23665763Sodium Bisulfite

생성물 2

HCID 6658Methyl MethacrylateHCID 170502-(Diethylamino)ethyl acrylate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

50 Grams of N,N-diethylaminoethyl methacrylate, 50 g. of methyl methacrylate, 1 g. of Dupanol ME, 1 g. of Emulphor ON-870, 6 g. of ethylene diacrylate, 1 g. of potassium persulfate, and 0.5 g. of sodium bisulfite are dissolved or mixed with 1,000 g. of water. This mixture is tumbled in a water bath at 60° C. for 24 hr. to obtain a crosslinked copolymer of methyl methacrylate and N,N-diethylaminoethyl acrylate. The crosslinked polymer is separated from the aqueous dispersion by the method described in Example 4.

후처리

  1. additionmixed with 1,000 g

출처 및 근거

ORD 기록
ord-efb2909c87374da8ab769c9d65862d66
출처 데이터셋
uspto-grants-1979_12
특허 번호
US04177255

연결된 노트

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