Di-tert-butyl dicarbonate → HCID 68477709, 화합물

HRID 1466485노트

반응식

HRID 1466485 반응식
[CH3:1][C:2]1[CH:3]=[C:4]2[C:8](=[C:9]([N+:11]([O-:13])=[O:12])[CH:10]=1)[NH:7][C:6]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[CH:5]2.[O:20](C(OC(C)(C)C)=O)[C:21]([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=O>CN(C1C=CN=CC=1)C>[C:21]([N:7]1[C:8]2[C:4](=[CH:3][C:2]([CH3:1])=[CH:10][C:9]=2[N+:11]([O-:13])=[O:12])[CH:5]=[C:6]1[C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=[O:20]

참가 물질

4

반응물 2

HCID 90495Di-tert-butyl dicarbonateHCID 68477399HCID 68477399, 화합물

생성물 1

HCID 68477709HCID 68477709, 화합물

시약·촉매·용매 1

HCID 142844-(Dimethylamino)pyridine촉매

실험 절차

5-Methyl-7-nitro-2-phenyl-1H-indole prepared in Preparation 24, (BOC)2O and DMAP were reacted according to the same procedure as Preparation 23 to give the title compound.

후처리

  1. customwere reacted
  2. customaccording to the same procedure as Preparation 23

출처 및 근거

ORD 기록
ord-a57c76f8555b474b9a2551e1adf6055b
출처 데이터셋
uspto-grants-2015_04
특허 번호
US09000028B2

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