Hydrochloric Acid → HCID 19830594, 화합물

HRID 1493106

반응식

HRID 1493106 반응식
Cl[C:2]1[CH:7]=[CH:6][C:5]([NH:8][S:9]([CH3:12])(=[O:11])=[O:10])=[CH:4][C:3]=1[N+:13]([O-])=O.[C:16]([C:20]1[CH:25]=[CH:24][C:23]([OH:26])=[CH:22][CH:21]=1)([CH3:19])([CH3:18])[CH3:17].C(=O)([O-])[O-].[K+].[K+].Cl>O.C1(C)C(C)=CC=CC=1.COCCOCCOC>[C:16]([C:20]1[CH:21]=[CH:22][C:23]([O:26][C:2]2[CH:7]=[CH:6][C:5]([NH:8][S:9]([CH3:12])(=[O:11])=[O:10])=[CH:4][C:3]=2[NH2:13])=[CH:24][CH:25]=1)([CH3:19])([CH3:17])[CH3:18]

참가 물질

8

반응물 4

HCID 313Hydrochloric AcidHCID 73934-tert-ButylphenolHCID 11430Potassium CarbonateHCID 3755760N-(4-chloro-3-nitrophenyl)methanesulfonamide

생성물 1

HCID 19830594HCID 19830594, 화합물

시약·촉매·용매 3

HCID 962Water용매HCID 7237O-Xylene용매HCID 8150Diglyme용매

실험 절차

N-(4-chloro-3-nitrophenyl)methanesulphonamide (50 g, 0.2 mole), 4-t-butylphenol (33 g, 0.22 mole), potassium carbonate (62.1 g, 0.45 mole) and diglyme (50 ml) were heated and stirred at 165°-170° for 24 hr. The mixture was cooled to 110° and xylene (150 ml) followed by a mixture of 10M-hydrochloric acid (55 ml) and water (130 ml) added.

후처리

  1. temperatureThe mixture was cooled to 110°
  2. additionadded

출처 및 근거

ORD 기록
ord-ae428aa6bb0d4d399b66e410cbcd4fe2
출처 데이터셋
uspto-grants-1991_06
특허 번호
US05021333

연결된 노트

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