Hydrochloric Acid → Phenyl octanoate

HRID 1599522노트

반응식

HRID 1599522 반응식
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:8](O)(=[O:16])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].S(=O)=O.Cl>S(Cl)(Cl)=O>[C:8]([O:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)(=[O:16])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]

참가 물질

6

반응물 4

HCID 313Hydrochloric AcidHCID 379Octanoic AcidHCID 996PhenolHCID 1119Sulfur Dioxide

생성물 1

HCID 229895Phenyl octanoate

시약·촉매·용매 1

HCID 24386Thionyl Chloride용매

실험 절차

The ester was prepared by slowly adding thionyl chloride (10 ml) to a mixture of pure phenol (6.5 g) and octanoic acid (10 g). The reaction mixture was warmed to drive off the sulfur dioxide and hydrogen chloride gases. The crude mixture was distilled at 95°-100° C./5 mmHg.

후처리

  1. temperatureThe reaction mixture was warmed
  2. distillationThe crude mixture was distilled at 95°-100° C./5 mmHg

출처 및 근거

ORD 기록
ord-2c67f39815a040c1b539b782c2b2c497
출처 데이터셋
uspto-grants-1998_04
특허 번호
US05741821

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