Hydrochloric Acid → 1,1-Cyclopentanedimethanamine

HRID 1607617

반응식

HRID 1607617 반응식
Cl.Cl.[C:3]1([CH2:10][NH2:11])([CH2:8][NH2:9])[CH2:7][CH2:6][CH2:5][CH2:4]1.Cl>[OH-].[Na+].Cl[Pt-2](Cl)(Cl)Cl.[K+].[K+]>[C:3]1([CH2:10][NH2:11])([CH2:8][NH2:9])[CH2:7][CH2:6][CH2:5][CH2:4]1

참가 물질

5

반응물 2

HCID 313Hydrochloric AcidHCID 1317151911,1-Cyclopentanedimethanamine, dihydrochloride

생성물 1

HCID 4325931,1-Cyclopentanedimethanamine

시약·촉매·용매 2

HCID 61440Dipotassium tetrachloroplatinate촉매HCID 14798Sodium Hydroxide용매

실험 절차

A 2.01 g portion of this amine derivative was dissolved in 20 ml of 1N sodium hydroxide, the pH was adjusted to 7.0 with hydrochloric acid and 4.15 g of potassium tetrachloroplatinate was added. The mixture was stirred for 4 hours, then the solid was collected, washed with water and dried, giving 2.1 g of 1,1-cyclopentanedimethanamine, compound with platinum chloride.

후처리

  1. additionwas added
  2. customthe solid was collected
  3. washwashed with water
  4. customdried

출처 및 근거

ORD 기록
ord-a83a4d882d5a4787913fa67342450b91
출처 데이터셋
uspto-grants-1989_09
특허 번호
US04866092

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