Hydrochloric Acid → HCID 54392493, 화합물

HRID 1660541노트

반응식

HRID 1660541 반응식
[CH2:1]([C:4]1[CH:5]=[C:6]([C:11]([C:14]2[CH:19]=[CH:18][C:17]([OH:20])=[C:16]([CH2:21][CH:22]=[CH2:23])[CH:15]=2)([CH3:13])[CH3:12])[CH:7]=[CH:8][C:9]=1[OH:10])[CH:2]=[CH2:3].[OH-].[K+].Cl>>[CH:21]([C:16]1[CH:15]=[C:14]([C:11]([C:6]2[CH:7]=[CH:8][C:9]([OH:10])=[C:4]([CH:1]=[CH:2][CH3:3])[CH:5]=2)([CH3:12])[CH3:13])[CH:19]=[CH:18][C:17]=1[OH:20])=[CH:22][CH3:23]

참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 14797Potassium HydroxideHCID 74457Phenol, 4,4'-(1-methylethylidene)bis(2-(2-propen-1-yl)-

생성물 1

HCID 54392493HCID 54392493, 화합물

실험 절차

2,2-Bis(3-allyl-4-hydroxyphenyl)propane (1 mole) was mixed with potassium hydroxide pellets (2.2 moles) and the mixture was stirred and heated at 110° for 30 minutes. The mixture was cooled, neutralised with dilute hydrochloric acid, and the product was extracted to give methylene chloride. The solution was dried and evaporated to give substantially pure 2,2-bis(3-(1-propenyl)-4-hydroxyphenyl)propane.

후처리

  1. temperatureheated at 110° for 30 minutes
  2. temperatureThe mixture was cooled
  3. extractionthe product was extracted
  4. customto give methylene chloride
  5. customThe solution was dried
  6. customevaporated

출처 및 근거

ORD 기록
ord-e483e07df4414dc0bf7f15894c8d1bb4
출처 데이터셋
uspto-grants-1981_12
특허 번호
US04308367

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