2-Amino-5-Nitrothiazole → 3-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide

HRID 1701833

반응식

HRID 1701833 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7](Cl)=[O:8])([O-:3])=[O:2].[NH2:13][C:14]1[S:15][C:16]([N+:19]([O-:21])=[O:20])=[CH:17][N:18]=1>N1C=CC=CC=1>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7]([NH:13][C:14]1[S:15][C:16]([N+:19]([O-:21])=[O:20])=[CH:17][N:18]=1)=[O:8])([O-:3])=[O:2]

참가 물질

4

반응물 2

HCID 84862-Amino-5-NitrothiazoleHCID 8495Benzoyl chloride, 3-nitro-

생성물 1

HCID 2989303-nitro-N-(5-nitro-1,3-thiazol-2-yl)benzamide

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

By following the procedure of the first part of Example 1, but using m-nitrobenzoyl chloride (27.8 g), 2-amino-5-nitrothiazole (21.8 g) and pyridine (100 ml), there was obtained 3-nitro-N-(5-nitro-2-thiazolyl)benzamide, m.pt 200°-201°, after recrystallisation from acetic acid.

출처 및 근거

ORD 기록
ord-869f3175addf4932a6aa8edebdad26e4
출처 데이터셋
uspto-grants-1983_04
특허 번호
US04379156

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