Dichloromethane → 1-isocyano-2-phenylbenzene
반응식
[C:1]1([C:7]2[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=2[NH2:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:14](Cl)Cl.[OH-].[Na+]>[Cl-].C([N+](CC)(CC)CC)C1C=CC=CC=1.C(Cl)(Cl)Cl>[C:1]1([C:7]2[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=2[N+:9]#[C-:14])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1참가 물질
6
실험 절차
A reaction flask was charged with 17 g (0.1 mole) of 2-phenylaniline, 20 ml of methylene chloride, 15 ml of chloroform, 30 ml of 50% aqueous sodium hydroxide, and 200 mg of benzyltriethylammonium chloride. The procedure of Example 1 was followed, yielding 6 g of a thick oil, whose structure was confirmed by mass spectroscopy as that indicated by the above title.
출처 및 근거
- ORD 기록
- ord-f35a71179c054e06a5d038277d5cd936
- 출처 데이터셋
- uspto-grants-1983_04
- 특허 번호
- US04380468
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