Acetone → N-isopropyl-N-(3,4-dichlorostyryl)acetamidine

HRID 1706095노트

반응식

HRID 1706095 반응식
C(NC(=NS([CH:11]=[CH:12][C:13]1[CH:18]=[CH:17][C:16]([Cl:19])=[C:15]([Cl:20])[CH:14]=1)(=O)=O)C)(C)C.[OH-].[Na+].C[N:24]([CH:33]=[CH:34]C1C=CC([N+]([O-])=O)=CC=1)[C:25](=[NH:32])[C:26]1C=CC=CC=1.[CH3:44]C(C)=O>CS(C)=O>[CH:33]([N:24]([CH:11]=[CH:12][C:13]1[CH:18]=[CH:17][C:16]([Cl:19])=[C:15]([Cl:20])[CH:14]=1)[C:25](=[NH:32])[CH3:26])([CH3:34])[CH3:44]

참가 물질

6

반응물 4

HCID 180AcetoneHCID 14798Sodium HydroxideHCID 54226858HCID 54226858, 화합물HCID 178465746N-isopropyl-N'-(3,4-dichlorostyrylsulfonyl)acetamidine

생성물 1

HCID 54420898N-isopropyl-N-(3,4-dichlorostyryl)acetamidine

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매

실험 절차

Treating N-isopropyl-N'-(3,4-dichlorostyrylsulfonyl)acetamidine with aqueous sodium hydroxide in acetone or dimethylsulfoxide according to the procedure of Example 32 (c) provides N-isopropyl-N-(3,4-dichlorostyryl)acetamidine.

출처 및 근거

ORD 기록
ord-6a0956ccb9924c94be229c6e678c2796
출처 데이터셋
uspto-grants-1980_06
특허 번호
US04206142

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