Water → HCID 21471814, 화합물
반응식
[S:1]1[C:5]2[CH2:6][NH:7][CH2:8][CH2:9][CH2:10][C:4]=2[CH:3]=[CH:2]1.N1C=CC=CC=1.[C:17](OC(=O)C)(=[O:19])[CH3:18].O>C(Cl)(Cl)Cl>[C:17]([N:7]1[CH2:8][CH2:9][CH2:10][C:4]2[CH:3]=[CH:2][S:1][C:5]=2[CH2:6]1)(=[O:19])[CH3:18]참가 물질
6
실험 절차
To a mixture of 4 g of 5,6,7,8-tetrahydro-4H-thieno[2,3-c]azepine and 4 g of pyridine in 20 ml of chloroform was added 4.1 g of acetic anhydride under ice-cooling and the mixture was stirred at room temperature for an hour. The mixture was poured into water and extracted with chloroform. The extract was washed with water, dried and concentrated to give 4 g of 7-acetyl-5,6,7,8-tetrahydro-4H-thieno[2,3-c]azepine as an oil.
후처리
- temperaturecooling
- extractionextracted with chloroform
- washThe extract was washed with water
- customdried
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-49249ce58a8e425392a583ab3b9cd281
- 출처 데이터셋
- uspto-grants-1996_07
- 특허 번호
- US05532240
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