2-Ethylhexanoic Acid → Cobalt octoate

HRID 1757015

반응식

HRID 1757015 반응식
[CH2:1]([CH:3]([CH2:7][CH2:8][CH2:9][CH3:10])[C:4]([OH:6])=[O:5])[CH3:2].[OH-].[Na+].[Co:13]>[Pt]>[CH3:10][CH2:9][CH2:8][CH2:7][CH:3]([C:4]([O-:6])=[O:5])[CH2:1][CH3:2].[CH3:10][CH2:9][CH2:8][CH2:7][CH:3]([C:4]([O-:6])=[O:5])[CH2:1][CH3:2].[Co+2:13]

참가 물질

5

반응물 3

HCID 86972-Ethylhexanoic AcidHCID 14798Sodium HydroxideHCID 104730Cobalt2회

생성물 1

HCID 8696Cobalt octoate

시약·촉매·용매 1

HCID 23939Platinum촉매

실험 절차

The electrochemical reaction was carried out in a reaction cell containing 20.0 g (0.138 mole) of 2-ethylhexanoic acid, 10.0 g mineral spirits and 40.0 g of 0.1N sodium hydroxide. A cobalt rod was used as the anode and platinum foil as the cathode. The connections were made and direct current was passed through the cell. After passing 14,645 coulombs of electricity, the electrosynthesis process was terminated and the weight of the cobalt consumed in the reaction was determined. 3.68 g (0.062 mole) cobalt was consumed. The organics were separated from the aqueous phase and were dried under reduced pressure resulting in a violet solution of cobalt octoate in mineral spirits that contained 10.1% cobalt.

후처리

  1. customThe electrochemical reaction
  2. customthe electrosynthesis process was terminated
  3. customthe weight of the cobalt consumed in the reaction
  4. customThe organics were separated from the aqueous phase
  5. customwere dried under reduced pressure

출처 및 근거

ORD 기록
ord-16eca5b5f4e2456fa66ed1b7086cd6fd
출처 데이터셋
uspto-grants-1995_08
특허 번호
US05443698

연결된 노트

불러오는 중…