Bromide ion → HCID 13747683, 화합물

HRID 1762538

반응식

HRID 1762538 반응식
[OH:1][C:2]([CH3:20])([CH3:19])[CH2:3][CH2:4][CH2:5][CH2:6][N:7]1[C:15]2[C:14](=[O:16])[NH:13][C:12](=[O:17])[N:11]([CH3:18])[C:10]=2[N:9]=[CH:8]1.IC.[CH3:23]N1C(=O)C2N(CCCCC(=O)C)C=NC=2N(C)C1=O.C[Mg]Cl.[Br-].CN1C(=O)C2N(CCCC=C(C)C)C=NC=2N(C)C1=O>CCOCC>[OH:1][C:2]([CH3:20])([CH3:19])[CH2:3][CH2:4][CH2:5][CH2:6][N:7]1[C:15]2[C:14](=[O:16])[N:13]([CH3:23])[C:12](=[O:17])[N:11]([CH3:18])[C:10]=2[N:9]=[CH:8]1

참가 물질

8

반응물 6

HCID 259Bromide ionHCID 6328Methyl iodideHCID 65599LomifyllineHCID 13747680HCID 13747680, 화합물HCID 20041125HCID 20041125, 화합물HCID 178418332HCID 178418332, 화합물

생성물 1

HCID 13747683HCID 13747683, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

Alternatively, it was possible to prepare the compound, inter alia, from 7-(5-hydroxy-5-methylhexyl)-3-methylxanthine (Example 1b) and iodomethane analogously to Example 3, from 1,3-dimethyl-7-(5-oxohexyl)-xanthine and methylmagnesium chloride or bromide in anhydrous ether analogously to Example 9, and from 1,3-dimethyl-7-(5-methyl-4-hexenyl)-xanthine by acid-catalyzed hydration analogously to Example 14.

후처리

  1. customto prepare the compound, inter alia

출처 및 근거

ORD 기록
ord-590b90e31e1c4538baeea3ad2f472939
출처 데이터셋
uspto-grants-1989_05
특허 번호
US04833146

연결된 노트

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