4-tert-Butylcyclohexanol → 4-Tert-butylcyclohex-1-ene

HRID 1828330

반응식

HRID 1828330 반응식
[C:1]([CH:5]1[CH2:10][CH2:9][CH:8](O)[CH2:7][CH2:6]1)([CH3:4])([CH3:3])[CH3:2].OS([O-])(=O)=O.[K+].C(OC(=O)C)C.OS([O-])(=O)=O.[K+]>>[C:1]([CH:5]1[CH2:10][CH2:9][CH:8]=[CH:7][CH2:6]1)([CH3:4])([CH3:3])[CH3:2]

참가 물질

4

반응물 3

HCID 73914-tert-ButylcyclohexanolHCID 516920Potassium bisulfateHCID 86585043ethylacetate KHSO4

생성물 1

HCID 166884-Tert-butylcyclohex-1-ene

반응 조건

온도
95 °C

실험 절차

20 g 4-t-butyl-1-cyclohexanol are mixed with 17 g KHSO4 and stirred for one week at 95° C. After the addition of ethylacetate KHSO4 is filtered off. Ethylacetate is evaporated and the product obtained by fractional distillation.

후처리

  1. filtrationis filtered off
  2. customEthylacetate is evaporated
  3. customthe product obtained by fractional distillation

출처 및 근거

ORD 기록
ord-af0b71c7642b4961a781a860d53df6c6
출처 데이터셋
uspto-grants-2006_06
특허 번호
US07057059B2

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