Hydrochloric Acid → Sodium 1,1,3,3,3-pentafluoro-2-hydroxypropane-1-sulfonate
반응식
[F:1][C:2]([F:19])([S:15]([O-:18])(=[O:17])=[O:16])[CH:3]([O:8]C(=O)C(C)(C)C)[C:4]([F:7])([F:6])[F:5].[Na+:20].[OH-].[Na+].Cl>CO>[F:19][C:2]([F:1])([S:15]([O-:18])(=[O:16])=[O:17])[CH:3]([OH:8])[C:4]([F:5])([F:7])[F:6].[Na+:20]참가 물질
5
실험 절차
Ester hydrolysis reaction was effected using sodium 1,1,3,3,3-pentafluoro-2-(pivaloyloxy)propanesulfonate, which was prepared according to the formulation described in JP-A 2007-145797, and a sodium hydroxide aqueous solution in methanol. After the completion of reaction, hydrochloric acid was added to turn the reaction system from neutral to weakly acidic. The aqueous solution was directly used in the subsequent reaction.
후처리
- customwas prepared
- additionwas added
- customThe aqueous solution was directly used in the subsequent reaction
출처 및 근거
- ORD 기록
- ord-116a2f7ce61747d4b102643fe2f87669
- 출처 데이터셋
- uspto-grants-2012_05
- 특허 번호
- US08173354B2
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