Allyl isocyanate → 4-Isothiocyanatophenyl prop-2-en-1-ylcarbamate

HRID 1974227

반응식

HRID 1974227 반응식
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[C:9]=[S:10])=[CH:4][CH:3]=1.[CH2:11]([N:14]=[C:15]=[O:16])[CH:12]=[CH2:13]>C(Cl)(Cl)Cl.C(N(CC)CC)C.C([O-])(=O)CCCCCCCCCCC.C([O-])(=O)CCCCCCCCCCC.C([Sn+2]CCCC)CCC>[CH2:11]([NH:14][C:15]([O:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[C:9]=[S:10])=[CH:4][CH:3]=1)=[O:16])[CH:12]=[CH2:13]

참가 물질

6

반응물 2

HCID 15123Allyl isocyanateHCID 102208Phenol, 4-isothiocyanato-

생성물 1

HCID 214890044-Isothiocyanatophenyl prop-2-en-1-ylcarbamate

시약·촉매·용매 3

HCID 8471Triethylamine촉매HCID 9809426Di-n-butyldilauryltin촉매HCID 6212Chloroform용매

실험 절차

By a procedure similar to that of Example I, the above compound (11.1 g.) in the form of a waxy solid, was prepared from 9.1 g. (0.06 m.) of p-hydroxyphenylisothiocyanate and 5.0 g. (0.06 m.) of allylisocyanate, using 35 mls. of chloroform as a solvent and 3 drops each of triethylamine and dibutyltin dilaurate as catalysts.

후처리

  1. customBy a procedure similar to that of Example I, the above compound (11.1 g.) in the form of a waxy solid, was prepared from 9.1 g

출처 및 근거

ORD 기록
ord-692abc3ca1aa48bc9083b601ebe9fb96
출처 데이터셋
uspto-grants-1976_12
특허 번호
US04000253

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