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Ethylene → Cyclohexane, [(trichlorosilyl)methyl]-

HRID 1981056
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HRID 1981056 반응식
[Cl:1][SiH:2]([Cl:4])[Cl:3].[CH3:5][C:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH:7]=1.C=C>C(Cl)(Cl)Cl>[Cl:1][Si:2]([CH2:5][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1)([Cl:4])[Cl:3]
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참가 물질

5

반응물 3

HCID 6325EthyleneHCID 115741-MethylcyclohexeneHCID 24811Trichlorosilane

생성물 1

HCID 87618Cyclohexane, [(trichlorosilyl)methyl]-

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

A mixture of 20 ml trichlorosilane, 25 ml chloroform, 8.1 g 1-methylcyclohexene and 0.055 g (phenazine)PtCl2 (C2H4) was refluxed and stirred under nitrogen for 6 days. Distillation of the reaction mixture afforded 2.2 g of trichlorosilylmethylcyclohexane C6H11CH2SiCl3 which was characterized by its mass and NMR spectra.

후처리

  1. temperaturewas refluxed
  2. distillationDistillation of the reaction mixture

출처 및 근거

ORD 기록
ord-6e4cca18cbb14fea847c56c5f0e2364c
출처 데이터셋
uspto-grants-1985_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04511715

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