Ammonia → 3-Phenoxybenzamide

HRID 2052137

반응식

HRID 2052137 반응식
[NH3:1].[O:2]([C:9]1[CH:10]=[C:11]([CH:15]=[CH:16][CH:17]=1)[C:12](Cl)=[O:13])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>C(Cl)(Cl)Cl>[O:2]([C:9]1[CH:10]=[C:11]([CH:15]=[CH:16][CH:17]=1)[C:12]([NH2:1])=[O:13])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 222AmmoniaHCID 27603413-Phenoxybenzoyl chloride

생성물 1

HCID 166186253-Phenoxybenzamide

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

Saturated with anhydrous ammonia a solution containing 23 g (0.1 mole) of 3-phenoxybenzoyl chloride and 250 ml of AR chloroform. Continued stirring for 30 min., chilled to 0° and filtered. The product was pulverised, triturated in cold water and oven-dried to give 21.3 g, m.p. 127°-128°.

후처리

  1. temperaturechilled to 0°
  2. filtrationfiltered
  3. customtriturated in cold water
  4. customoven-dried
  5. customto give 21.3 g, m.p. 127°-128°

출처 및 근거

ORD 기록
ord-a39fde958b4e4272b8722604470a7011
출처 데이터셋
uspto-grants-1980_01
특허 번호
US04182881

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