Piperonal → Ilepcimide
반응식
O=Cc1ccc2c(c1)OCO2.O=C(O)CC(=O)N1CCCCC1>NCc1ccccc1.O=C(O)C(F)(F)F.CN(C)c1ccncc1.CN(C)C=O>O=C(/C=C/c1ccc2c(c1)OCO2)N1CCCCC1참가 물질
6
반응 조건
- 온도
- 50 °C
후처리
- temperatureThe product mixture was cooled to 25 °C.
- filtrationFiltered through a pad of celite · Organic 상 유지
- wash"The celite was washed with ethyl acetate (3 x 1 mL)."
- concentrationThe filtrate was concentrated under reduced pressure
- additionA 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.
출처 및 근거
- ORD 기록
- ord-fbf96c68eb8d41da8e80972be2e70ec1
- 출처 데이터셋
- Transfer learning optimization of 26 decarboxylative olefination reactions
반응 노트
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