Acetic Acid → HCID 75985013, 화합물
반응식
Br[CH2:2][C:3]([O:11][CH3:12])=[CH:4][C:5](=[O:10])[C:6]([Cl:9])([Cl:8])[Cl:7].[C:13]([O-:16])(=[O:15])[CH3:14].[K+].C(O)(=O)C>[Br-].C([N+](CCCC)(CCCC)CCCC)CCC.C(#N)C>[C:13]([O:16][CH2:2][C:3]([O:11][CH3:12])=[CH:4][C:5](=[O:10])[C:6]([Cl:9])([Cl:8])[Cl:7])(=[O:15])[CH3:14]참가 물질
6
실험 절차
29.6 g (0.1 mol) of 5-bromo-1,1,1-trichloro-4-methoxypent-3-en-2-one, 17 g of potassium acetate, 5 g of tetrabutylammonium bromide and 8 g of acetic acid were stirred at 40° C. in 300 ml of acetonitrile for 16 h. The mixture was concentrated under reduced pressure, and the water was added to the residue. The product was extracted with ethyl acetate, the organic phase was washed with water and the solvent was removed completely under reduced pressure.
후처리
- concentrationThe mixture was concentrated under reduced pressure
- additionthe water was added to the residue
- extractionThe product was extracted with ethyl acetate
- washthe organic phase was washed with water
- customthe solvent was removed completely under reduced pressure
출처 및 근거
- ORD 기록
- ord-d4988016eb784893b02484463198a10d
- 출처 데이터셋
- uspto-grants-2012_10
- 특허 번호
- US08299260B2
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