Di-tert-butyl dicarbonate → HCID 68477709, 화합물

HRID 2089573노트

반응식

HRID 2089573 반응식
[CH3:1][C:2]1[CH:3]=[C:4]2[C:8](=[C:9]([N+:11]([O-:13])=[O:12])[CH:10]=1)[NH:7][C:6]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[CH:5]2.[O:20](C(OC(C)(C)C)=O)[C:21]([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=O>CN(C1C=CN=CC=1)C>[C:21]([N:7]1[C:8]2[C:4](=[CH:3][C:2]([CH3:1])=[CH:10][C:9]=2[N+:11]([O-:13])=[O:12])[CH:5]=[C:6]1[C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=[O:20]

참가 물질

4

반응물 2

HCID 90495Di-tert-butyl dicarbonateHCID 68477399HCID 68477399, 화합물

생성물 1

HCID 68477709HCID 68477709, 화합물

시약·촉매·용매 1

HCID 142844-(Dimethylamino)pyridine촉매

실험 절차

5-Methyl-7-nitro-2-phenyl-1H-indole prepared in Preparation 24, (BOC)2O and DMAP were reacted according to the same procedure as Preparation 23 to give the title compound.

후처리

  1. customwere reacted
  2. customaccording to the same procedure as Preparation 23

출처 및 근거

ORD 기록
ord-b540a8308a694a92a8ccfecf40504f4c
출처 데이터셋
uspto-grants-2013_05
특허 번호
US08436038B2

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