Hydrochloric Acid → HCID 73198280, 화합물
반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[C:10]([O:12][CH3:13])[CH:11]=1)[C:8](=[O:14])[CH2:7][CH2:6]2.C([O:19][N:20]=O)CCC.Cl>CO>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[C:10]([O:12][CH3:13])[CH:11]=1)[C:8](=[O:14])[C:7](=[N:20][OH:19])[CH2:6]2참가 물질
5
반응 조건
- 온도
- 40 °C
실험 절차
To a solution of 5,7-Dimethoxy-indan-1-one (8.7 g, 45.26 mmol) in the methanol (80 ml) was added n-butylnitrite (6.13 ml, 49.78 mmol) followed by concentrated HCl (4.4 ml). The solution was stirred at 40° C. for one hour during which time a precipitate was formed. The precipitate was collected and dried to yield product as a yellow solid (10 g, 99%). LC-MS: m/e 222 (MH+).
후처리
- customwas formed
- customThe precipitate was collected
- customdried
출처 및 근거
- ORD 기록
- ord-356eb2a3bfd741db970fb5c55ad776de
- 출처 데이터셋
- uspto-grants-2009_08
- 특허 번호
- US07572809B2
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