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Water → HCID 67313923, 화합물

HRID 2179720
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인쇄 미리보기

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HRID 2179720 반응식
[H-].[Na+].[ClH:3].[N:4]12[CH2:11][CH2:10][CH:7]([CH2:8][CH2:9]1)[C@@H:6]([NH:12][C:13]([C:15]1[O:16][C:17]3[C:23]([C:24]4[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=4[O:30][CH3:31])=[CH:22][CH:21]=[CH:20][C:18]=3[CH:19]=1)=[O:14])[CH2:5]2.I[CH3:33].O>CN(C=O)C>[Cl-:3].[CH3:31][O:30][C:25]1[CH:26]=[CH:27][CH:28]=[CH:29][C:24]=1[C:23]1[C:17]2[O:16][C:15]([C:13]([NH:12][C@@H:6]3[CH:7]4[CH2:8][CH2:9][N+:4]([CH3:33])([CH2:11][CH2:10]4)[CH2:5]3)=[O:14])=[CH:19][C:18]=2[CH:20]=[CH:21][CH:22]=1
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 4

HCID 962WaterHCID 6328Methyl iodideHCID 24758Sodium hydrideHCID 67312922HCID 67312922, 화합물

생성물 1

HCID 67313923HCID 67313923, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

반응 조건

온도
-20 °C

실험 절차

60.5 mg (1.51 mmol) of sodium hydride (60% suspension in mineral oil) are added to a solution, cooled to −20° C., of 250 mg (0.61 mmol) of N-[(3R)-1-azabicyclo[2.2.2]oct-3-yl]-7-(2-methoxyphenyl)-1-benzofuran-2-carboxamide hydrochloride (Example 102) in 2.5 ml of DMF. After 30 min at room temperature and renewed cooling to −20° C., 33.9 μl (0.54 mmol) of iodomethane are added. After 18 h at room temperature, the reaction is stopped by adding water. The reaction mixture is purified by preparative HPLC. The product fractions are concentrated, codistilled with 1N hydrochloric acid, again concentrated and dried under high vacuum. 206 mg (79.7% of theory) of the title compound are obtained.

후처리

  1. waitAfter 18 h at room temperature
  2. customThe reaction mixture is purified by preparative HPLC
  3. concentrationThe product fractions are concentrated
  4. concentrationagain concentrated
  5. customdried under high vacuum

출처 및 근거

ORD 기록
ord-053da04254f04ef39d0d968de781d37c
출처 데이터셋
uspto-grants-2015_06
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09067931B2

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