Hydrogen Bromide → HCID 178515992, 화합물

HRID 2216339

반응식

HRID 2216339 반응식
[CH2:1]([C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([O:14]C)[N:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Br>O>[CH2:1]([C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([OH:14])[N:9]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

4

반응물 2

HCID 260Hydrogen BromideHCID 219422742-Benzyl-6-methoxypyridine

생성물 1

HCID 178515992HCID 178515992, 화합물수율 70.9%

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
100 °C

실험 절차

A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring in an oil bath at 100° C. for 7 hours. After standing to cool, 250 ml of water was added and the resulting crystals were filtered, washed with water and dried under reduced pressure, to give 38.9 g of the title compound.

후처리

  1. temperaturewas heated
  2. temperatureto cool
  3. filtrationthe resulting crystals were filtered
  4. washwashed with water
  5. customdried under reduced pressure

출처 및 근거

ORD 기록
ord-8432c46a7bbf42feb057a7de3b73cea2
출처 데이터셋
uspto-grants-2006_09
특허 번호
US07112593B2

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