Methyldichlorosilane → Silane, dichlorodecylmethyl-
반응식
[CH3:1][SiH:2]([Cl:4])[Cl:3].[CH2:5]=[CH:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>[H+].[H+].Cl[Pt-2](Cl)(Cl)(Cl)(Cl)Cl.CC(O)C>[CH3:1][Si:2]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])([Cl:4])[Cl:3]참가 물질
5
실험 절차
2.25 Parts of methyl dichlorosilane, 4.04 parts of 1-decene and a solution containing about 0.0005 part of chloroplatinic acid catalyst in 0.006 part of 2-propanol were charged to a reaction vessel and heated to about 100°-120° C. for six hours. The product was vacuum distilled at 110°-114° C. at 1-3 Torr. 4.7 Parts (94% yield) of methyl decyl dichlorosilane was obtained.
후처리
- additionwere charged to a reaction vessel
- temperatureheated to about 100°-120° C. for six hours
- distillationdistilled at 110°-114° C. at 1-3 Torr
출처 및 근거
- ORD 기록
- ord-111dd210d57e425787cb6ff3d4b6e9fa
- 출처 데이터셋
- uspto-grants-1982_10
- 특허 번호
- US04355062
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