Acetic Anhydride → Magnesium Acetate

HRID 224568

반응식

HRID 224568 반응식
O.O.O.O.[C:5]([O-:8])(=[O:7])[CH3:6].[Mg+2:9].[C:10]([O-:13])(=[O:12])[CH3:11].C(OC(=O)C)(=O)C>>[C:5]([O-:8])(=[O:7])[CH3:6].[Mg+2:9].[C:10]([O-:13])(=[O:12])[CH3:11]

참가 물질

3

반응물 2

HCID 7918Acetic AnhydrideHCID 134717Magnesium Acetate Tetrahydrate

생성물 1

HCID 8896Magnesium Acetate

실험 절차

Into a 300 ml. flask equipped with mechanical stirrer and a condenser, and maintained under a nitrogen atmosphere, were added 21.5 grams magnesium acetate tetrahydrate and 100 ml. acetic anhydride and the mixture was heated at the reflux temperature for 3 hours. After the mixture had cooled, the liquid was drawn off and the solid dried at 40° C. under a vacuum of 0.2 mm mercury for several hours to obtain anhydrous magnesium acetate.

후처리

  1. customflask equipped with mechanical stirrer and a condenser
  2. temperaturemaintained under a nitrogen atmosphere
  3. temperatureAfter the mixture had cooled
  4. dry with materialthe solid dried at 40° C. under a vacuum of 0.2 mm mercury for several hours

출처 및 근거

ORD 기록
ord-56af01c8ea0a44fa94837dac24bd83f2
출처 데이터셋
uspto-grants-1980_11
특허 번호
US04233253

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