Methanol → Methyl Benzoate

HRID 224949

반응식

C(C#N)(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:11](Cl)(=[O:18])C1C=CC=CC=1.S(=O)(=O)(O)O.[CH3:25][OH:26]>>[C:25]([O:18][CH3:11])(=[O:26])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

반응물 4

HCID 887Methanol

HCID 1118Sulfuric Acid

HCID 7412Benzoyl chloride

HCID 11953Phenylglyoxylonitrile

생성물 1

HCID 7150Methyl Benzoate

실험 절차

For example, when pure benzoyl cyanide (i.e., containing essentially no halide ion or halide ion source, such as benzoyl chloride) is reacted with concentrated sulfuric acid and then esterified by further reaction with methanol, the cyano group is cleaved and methyl benzoate is formed as follows: ##STR2##

출처 및 근거

ORD 기록: ord-3210b225ed214befa775d9f51e527f56
출처 데이터셋: uspto-grants-1980_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04234739

연결된 노트

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