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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Ammonium Acetate → 4-Piperidinamine, 1-(5-isoquinolinylsulfonyl)-

HRID 2291945
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HRID 2291945 반응식
[CH:1]1[C:10]2[CH:9]=[CH:8][CH:7]=[C:6]([S:11]([N:14]3[CH2:19][CH2:18][C:17](=O)[CH2:16][CH2:15]3)(=[O:13])=[O:12])[C:5]=2[CH:4]=[CH:3][N:2]=1.C([O-])(=O)C.[NH4+].C([BH3-])#[N:27].[Na+]>CO>[CH:1]1[C:10]2[CH:9]=[CH:8][CH:7]=[C:6]([S:11]([N:14]3[CH2:19][CH2:18][CH:17]([NH2:27])[CH2:16][CH2:15]3)(=[O:13])=[O:12])[C:5]=2[CH:4]=[CH:3][N:2]=1
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 517165Ammonium AcetateHCID 5003444Sodium cyanoborohydrideHCID 14326854HCID 14326854, 화합물

생성물 1

HCID 97960614-Piperidinamine, 1-(5-isoquinolinylsulfonyl)-

시약·촉매·용매 1

HCID 887Methanol용매

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온도
20 °C

실험 절차

To 50 ml of methanol were added 2.9 g of the thus obtained 1-(5-isoquinolinesulfonyl)-4-piperidone, 2.31 g of ammonium acetate and 0.63 g of sodium cyanoborohydride, followed by stirring at 20° C. for 24 hours. The methanol was removed under reduced pressure, and 100 ml of chloroform was added to the resultant product. Then, the mixture was washed twice with 50 ml each of water, washed once with 50 ml of a 50% aqueous sodium hydrogencarbonate solution, and dried with anhydrous sodium sulfate. The solvent was removed under reduced pressure to obtain a residue. The residue thus obtained was subjected to purification by silica gel column chromatography (Wacogel C-200, 150 g; solvent: chloroform) to obtain 2.39 g of 1-(5-isoquinolinesulfonyl)-4-aminopiperidine [Compound (51)]. Compound (51) was analyzed to give the following data.

후처리

  1. customThe methanol was removed under reduced pressure, and 100 ml of chloroform
  2. additionwas added to the resultant product
  3. washThen, the mixture was washed twice with 50 ml each of water
  4. washwashed once with 50 ml of a 50% aqueous sodium hydrogencarbonate solution
  5. dry with materialdried with anhydrous sodium sulfate
  6. customThe solvent was removed under reduced pressure
  7. customto obtain a residue
  8. customThe residue thus obtained
  9. customwas subjected to purification by silica gel column chromatography (Wacogel C-200, 150 g; solvent: chloroform)

출처 및 근거

ORD 기록
ord-dec27a263f2c4716b9579f239641bba7
출처 데이터셋
uspto-grants-1989_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04798897

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