Chlorodimethylsilane → HCID 13529574, 화합물
반응식
[CH2:1]([C:3]([CH2:9][CH3:10])=[C:4]([CH2:7][CH3:8])[CH2:5][CH3:6])[CH3:2].[CH3:11][SiH:12]([CH3:14])[Cl:13].[Al+3].[Cl-].[Cl-].[Cl-]>CCCCC>[CH2:1]([C:3]([Si:12]([CH3:14])([CH3:11])[Cl:13])([CH2:9][CH3:10])[CH:4]([CH2:7][CH3:8])[CH2:5][CH3:6])[CH3:2]참가 물질
5
실험 절차
2.1 g of tetraethylethylene, 2 ml (18 mmol) of dimethylchlorosilane and 200 mg of AlCl3 are reacted according to Example 1. After 2 hours, the reaction mixture is diluted with pentane and the precipitate is filtered off. The pentane is stripped from the filtrate in vacuo and the residue is distilled. This gives 2.8 g (80% of theory) of product as a colourless liquid. Boiling point=75°-80° C./0.195 mbar.
후처리
- filtrationthe precipitate is filtered off
- distillationthe residue is distilled
출처 및 근거
- ORD 기록
- ord-63aa4b82a32e498b9d7caa4d6112011f
- 출처 데이터셋
- uspto-grants-1989_01
- 특허 번호
- US04801719
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