2-Pyrrolidone → 1-Heptylpyrrolidin-2-one
반응식
[H-].[Na+].[NH:3]1[CH2:7][CH2:6][CH2:5][C:4]1=[O:8].Br[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>C1(C)C=CC=CC=1>[CH2:10]([N:3]1[CH2:7][CH2:6][CH2:5][C:4]1=[O:8])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]참가 물질
5
실험 절차
Following example 1, on refluxing 13 g of 50% oil dispersion of sodium hydride (6.5 g NaH, 0.27 M), 20.35 g (0.239 M) of azacyclopentan-2-one and 47.28 g (0.264M) of 1-bromoheptane in dry toluene for 21 hours was obtained 13.6 g (31%) of colorless oil; boiling point 115°-120°/0.6 mm.
출처 및 근거
- ORD 기록
- ord-6d4b840764c2478a868210492f255827
- 출처 데이터셋
- uspto-grants-1984_01
- 특허 번호
- US04424210
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