Water → 6'-Hydroxy-2'-(methoxycarbonylmethoxy)acetophenone
반응식
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([OH:8])[C:3]=1[C:9](=[O:11])[CH3:10].C(=O)([O-])[O-].[K+].[K+].Br[CH2:19][C:20]([O:22][CH3:23])=[O:21].O>CC(C)=O>[OH:1][C:2]1[C:3]([C:9](=[O:11])[CH3:10])=[C:4]([O:8][CH2:19][C:20]([O:22][CH3:23])=[O:21])[CH:5]=[CH:6][CH:7]=1참가 물질
6
실험 절차
To a mixture of 2′,6′-dihydroxyacetophenone (6 g) and potassium carbonate (5.72 g) in acetone (20 mL) was added methyl bromoacetate (3.73 mL), and the mixture was stirred at room temperature for 5 days. To the reaction mixture was added water, and the precipitated crystals were collected by filtration. The crystals were washed with water and dried under reduced pressure to give the title compound (7.89 g).
후처리
- filtrationthe precipitated crystals were collected by filtration
- washThe crystals were washed with water
- customdried under reduced pressure
출처 및 근거
- ORD 기록
- ord-9697439f8c5f4eaf8fdafdd370708a5d
- 출처 데이터셋
- uspto-grants-2009_07
- 특허 번호
- US07566699B2
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