Ethylenediamine → 2-(2-Dodecyl)-2-imidazoline

HRID 2352209

반응식

HRID 2352209 반응식
[C:1]([CH:3]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[CH3:4])#[N:2].[CH2:15](N)[CH2:16][NH2:17]>C(=S)=S>[CH3:4][CH:3]([C:1]1[NH:2][CH2:15][CH2:16][N:17]=1)[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

참가 물질

4

반응물 2

HCID 3301EthylenediamineHCID 1034242-Methyldodecanonitrile

생성물 1

HCID 146517992-(2-Dodecyl)-2-imidazoline수율 65%

시약·촉매·용매 1

HCID 6348Carbon Disulfide용매

실험 절차

19.53 g (100 mmoles) of 2-cyanododecane, 8.5ml (127 mmoles) of ethylenediamine and 0.5 ml of carbon disulfide are reacted according to Example 29 and the reaction mixture is worked up as mentioned therein. Distillation of the residue gives 15.5 g (65%) of the product.

후처리

  1. distillationDistillation of the residue

출처 및 근거

ORD 기록
ord-88eb195044d540eeb46b2c20959d9d81
출처 데이터셋
uspto-grants-1989_10
특허 번호
US04876249

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