Ethylenediamine → HCID 14651800, 화합물
반응식
[C:1]([C:3]([CH3:13])([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:4])#[N:2].[CH2:14](N)[CH2:15][NH2:16]>C(=S)=S>[CH3:4][C:3]([C:1]1[NH:2][CH2:14][CH2:15][N:16]=1)([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:13]참가 물질
4
실험 절차
18.32 g (100 mmoles) of 2-cyano-2-methyldecane, 8.5 ml (127 mmoles) of ethylenediamine and 0.5 ml of carbon disulfide are reacted according to Example 29 and the reaction mixture is worked up as mentioned therein. Distillation of the residue gives 13.91 g (62%) of the product.
후처리
- distillationDistillation of the residue
출처 및 근거
- ORD 기록
- ord-bdba5c0bbe55404592e9833eca563d7c
- 출처 데이터셋
- uspto-grants-1989_10
- 특허 번호
- US04876249
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