Hydrogen Bromide → 2,6-Diphenylpyridine hydrobromide

HRID 235609

반응식

HRID 235609 반응식
[BrH:1].[C:2]1([C:8]2[CH:13]=[CH:12][CH:11]=[C:10]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[N:9]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C1(C)C=CC=CC=1>[BrH:1].[C:14]1([C:10]2[CH:11]=[CH:12][CH:13]=[C:8]([C:2]3[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=3)[N:9]=2)[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1

참가 물질

4

반응물 2

HCID 260Hydrogen Bromide2회HCID 729202,6-Diphenylpyridine

생성물 1

HCID 202183212,6-Diphenylpyridine hydrobromide

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Hydrogen bromide gas is introduced into a solution of 30 g (0.130 mole) of 2,6-diphenylpyridine in 150 ml of toluene. The solid which forms is isolated by vacuum filtration. The filtrate is retreated with hydrogen bromide until no more solid is formed. The solid is then dried in vacuo. The product has a melting point of 161° C.-162° C.

후처리

  1. customThe solid which forms is isolated by vacuum filtration
  2. customis formed
  3. customThe solid is then dried in vacuo

출처 및 근거

ORD 기록
ord-60faa63473cd46718136fe30ba636c9d
출처 데이터셋
uspto-grants-1987_02
특허 번호
US04640831

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