Iodoethane → HCID 57448047, 화합물
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[Cl:1][C:2]1[C:7]([S:8]([CH3:11])(=[O:10])=[O:9])=[CH:6][CH:5]=[CH:4][C:3]=1[C:12]1[CH:17]=[CH:16][N:15]=[CH:14][CH:13]=1.I[CH2:19][CH3:20].[BH4-].[Na+]>C(O)C>[Cl:1][C:2]1[C:7]([S:8]([CH3:11])(=[O:10])=[O:9])=[CH:6][CH:5]=[CH:4][C:3]=1[C:12]1[CH2:13][CH2:14][N:15]([CH2:19][CH3:20])[CH2:16][CH:17]=1참가 물질
5
실험 절차
Preparation according to preparation 6: 4-[2-chloro-3-(methylsulfonyl)phenyl]-pyridine (1.77 g, 6.6 mmol), 1-iodoethane (5 ml), ethanol (40 ml), sodium borohydride (2.2 g, 58 mmol). Yield: 0.6 g. MS m/z (rel. intensity, 70 eV) 300 (M+, 24), 299 (M+, 71), 298 (33), 284 (bp), 110 (74).
후처리
- customPreparation
- customaccording to preparation 6
출처 및 근거
- ORD 기록
- ord-1eb187fad91a4eba80f5e97d46b6c574
- 출처 데이터셋
- uspto-grants-2010_07
- 특허 번호
- US07763639B2
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