Sodium Hydroxide → 2-Bromophenylhydrazine

HRID 2360490

반응식

HRID 2360490 반응식
Cl.[Br:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][NH2:10].[OH-].[Na+]>C1(C)C=CC=CC=1>[Br:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][NH2:10]

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 27239122-Bromophenylhydrazine hydrochloride

생성물 1

HCID 855832-Bromophenylhydrazine

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

15 g 2-bromophenylhydrazine hydrochloride are suspended in 400 ml of toluene and combined with 240 ml of 1 N sodium hydroxide solution. The mixture is stirred for 1 hour and the phases are separated. The organic phase is dried on magnesium sulphate and the solvents are eliminated in vacuo. The crude product thus obtained is further reacted directly.

후처리

  1. customthe phases are separated
  2. customThe organic phase is dried on magnesium sulphate

출처 및 근거

ORD 기록
ord-15172afbc4084c749fa1d4454ea24d19
출처 데이터셋
uspto-grants-2014_04
특허 번호
US08686022B2

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