Sodium amide → Hexamethyldisilazane

HRID 236425

반응식

HRID 236425 반응식
[CH3:1][Si:2]([CH3:9])([CH3:8])[O:3][Si:4]([CH3:7])([CH3:6])[CH3:5].[NH2-:10].[Na+:11]>C(OCC)C>[CH3:1][Si:2]([CH3:9])([CH3:8])[O-:3].[Na+:11].[CH3:1][Si:2]([NH:10][Si:4]([CH3:5])([CH3:6])[CH3:7])([CH3:9])[CH3:8]

참가 물질

5

반응물 2

HCID 24533Sodium amideHCID 24764Hexamethyldisiloxane

생성물 2

HCID 13838HexamethyldisilazaneHCID 23672319Sodium trimethylsilanolate

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

By product hexamethyldisiloxane in ethyl ether reacts with sodium amide to form sodium trimethylsilanolate and HMDS as follows: ##STR5##

출처 및 근거

ORD 기록
ord-875a1bf7e634459493370e67283ad6e0
출처 데이터셋
uspto-grants-1987_02
특허 번호
US04644076

연결된 노트

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