Ammonia → HCID 3046207, 화합물
반응식
[NH2-:1].[Na+].N.[Na].[CH2:5]([C:8]([CH2:12][CH2:13][CH3:14])(Cl)[C:9]#[CH:10])[CH2:6][CH3:7]>C(OCC)C>[CH2:5]([C:8]([NH2:1])([CH2:12][CH2:13][CH3:14])[C:9]#[CH:10])[CH2:6][CH3:7]참가 물질
6
실험 절차
To a suspension of sodium amide in liquid ammonia, prepared from 6.9 g of sodium and 250 ml of liquid ammonia, were added 17 g of 1,1-di-n-propyl-1-chloro-2-propyne in 50 ml of anhydrous ethyl ether. The operation of adding the chlorinated derivative lasted one hour. Stirring of the mixture was maintained for 2 hours and then 300 ml of anhydrous ethyl ether were added.
후처리
- additionThe operation of adding the chlorinated derivative
- temperaturewas maintained for 2 hours
출처 및 근거
- ORD 기록
- ord-9da5dec10eb545ba9883d896baae35ff
- 출처 데이터셋
- uspto-grants-1977_05
- 특허 번호
- US04026925
반응 노트
불러오는 중…