Dicyclohexylcarbodiimide → HCID 86665258, 화합물
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[CH3:1][O:2][C:3](=[O:11])[CH2:4][C@H:5]([CH3:10])[CH2:6][C:7](O)=[O:8].[CH3:12][Si:13]([CH3:18])([CH3:17])[CH2:14][CH2:15][OH:16].C1CCC(N=C=NC2CCCCC2)CC1.C(=O)(O)[O-].[Na+]>C(Cl)Cl.CN(C1C=CN=CC=1)C>[CH3:12][Si:13]([CH3:18])([CH3:17])[CH2:14][CH2:15][O:16][C:7](=[O:8])[CH2:6][C@@H:5]([CH3:10])[CH2:4][C:3]([O:2][CH3:1])=[O:11]참가 물질
7
실험 절차
To the solution of 3-(R)-Methyl-pentanedioic acid monomethyl ester in methylene chloride was added 2-Trimethylsilanyl-ethanol followed by DCC and DMAP and was stirred for 30 minutes. The reaction mixture was treated with sodium bicarbonate and methylene chloride. The product was purified by column chromatography.
후처리
- customThe product was purified by column chromatography
출처 및 근거
- ORD 기록
- ord-4d881d597abd4ad4b1db39f1a8013700
- 출처 데이터셋
- uspto-grants-2014_08
- 특허 번호
- US08809382B2
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