Methyl iodide → Methyl N-(2,6-dichlorobenzyl)dithiocarbamate

HRID 247409

반응식

[Cl:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([Cl:10])[C:3]=1[CH2:4][NH2:5].[C:11](=[S:13])=[S:12].I[CH3:15]>>[Cl:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([Cl:10])[C:3]=1[CH2:4][NH:5][C:11](=[S:13])[S:12][CH3:15]

참가 물질

반응물 3

HCID 6328Methyl iodide

HCID 6348Carbon Disulfide

HCID 485432Benzenemethanamine, 2,6-dichloro-

생성물 1

HCID 14049926Methyl N-(2,6-dichlorobenzyl)dithiocarbamate수율 32%

실험 절차

2,6-Dichlorobenzylamine (0.020 mol) was reacted with carbon disulfide (0.020 mol) and iodomethane (0.019 mol) substantially as described in Example 1B above to obtain 1.5 g (32%) white crystals: mp 47°.

출처 및 근거

ORD 기록: ord-f83dc7a65cf74d4d9c02b7a86857070d
출처 데이터셋: uspto-grants-1987_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04707488

연결된 노트

불러오는 중…