p-Aminoacetophenone → HCID 178466740, 화합물

HRID 24785

반응식

HRID 24785 반응식
C([N:4]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6](=[C:13](OCC)[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[C:5]1=[O:23])(=O)C.[CH3:24][C:25]([C:27]1[CH:32]=[CH:31][C:30]([NH2:33])=[CH:29][CH:28]=1)=[O:26].[OH-].[Na+]>CN(C=O)C.CO>[C:25]([C:27]1[CH:32]=[CH:31][C:30]([NH:33]/[C:13](=[C:6]2\[C:5](=[O:23])[NH:4][C:12]3[C:7]\2=[CH:8][CH:9]=[CH:10][CH:11]=3)/[C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=2)=[CH:29][CH:28]=1)(=[O:26])[CH3:24]

참가 물질

6

반응물 3

HCID 7468p-AminoacetophenoneHCID 14798Sodium HydroxideHCID 542378881-Acetyl-3-(1-ethoxy-1-phenylmethylidene}-2-indolinone

생성물 1

HCID 178466740HCID 178466740, 화합물

시약·촉매·용매 2

HCID 887Methanol용매HCID 6228Dimethylformamide용매

실험 절차

Prepared analogously to Example 1 from 1-acetyl-3-(1-ethoxy-1-phenyl-methylidene)-2-indolinone and 4-aminoacetophenone in DMF and subsequent treatment with sodium hydroxide solution in methanol.

출처 및 근거

ORD 기록
ord-8ebc37f197b242d28ad364d27430db3c
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06855710B2

연결된 노트

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