Propanal → HCID 178457072, 화합물

HRID 24865

반응식

HRID 24865 반응식
Cl.[NH2:2][CH2:3][C:4]1[CH:9]=[CH:8][C:7]([NH:10]/[C:11](=[C:18]2\[C:19](=[O:30])[NH:20][C:21]3[C:26]\2=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][CH:22]=3)/[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:6][CH:5]=1.[CH:31](=O)[CH2:32][CH3:33].C([BH3-])#N.[Na+]>CO>[CH2:31]([NH:2][CH2:3][C:4]1[CH:5]=[CH:6][C:7]([NH:10]/[C:11](=[C:18]2\[C:19](=[O:30])[NH:20][C:21]3[C:26]\2=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][CH:22]=3)/[C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)=[CH:8][CH:9]=1)[CH2:32][CH3:33]

참가 물질

5

반응물 3

HCID 527PropanalHCID 5003444Sodium cyanoborohydrideHCID 178479182HCID 178479182, 화합물

생성물 1

HCID 178457072HCID 178457072, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Prepared analogously to Example 159 from (Z)-3-[1-(4-aminomethyl-phenylamino)-1-phenyl-methylidene]-5-nitro-2-indolinone-hydrochloride, propionaldehyde and sodium cyanoborohydride in methanol.

출처 및 근거

ORD 기록
ord-59136c92f1894dfca344be0da35b67bc
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06855710B2

연결된 노트

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