Hydrochloric Acid → n-Nonadecyl-n-tetradecyl-n-decylmethylchloride

HRID 2591노트

반응식

HRID 2591 반응식
[CH2:1]([C:20]([CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH3:45])([CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31])O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[Cl-:46].[Ca+2].[Cl-].Cl>C(Cl)Cl>[CH2:1]([C:20]([Cl:46])([CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH3:45])[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 5284359Calcium ChlorideHCID 19690417n-Nonadecyl-n-tetradecyl-n-decylcarbinol

생성물 1

HCID 19690413n-Nonadecyl-n-tetradecyl-n-decylmethylchloride

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

One mole of n-nonadecyl-n-tetradecyl-n-decylcarbinol is added to 0.2 liters of methylene chloride and 0.32 moles calcium chloride. Approximately 1.5 moles of HCl gas is slowly bubbled through the solution. The product mixture is then washed with 1 liter of a 10% sodium carbonate solution. The organic layer is dried with magnesium sulfate and the methylene chloride is evaporated off to give n-nonadecyl-n-tetradecyl-n-decylmethylchloride.

후처리

  1. washThe product mixture is then washed with 1 liter of a 10% sodium carbonate solution
  2. dry with materialThe organic layer is dried with magnesium sulfate
  3. customthe methylene chloride is evaporated off

출처 및 근거

ORD 기록
ord-5357024e5ff4448eabdc6f4dbebdfb2c
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05728907

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