Dimethylamine → 2-(Aminomethylidene)-2,3-dihydro-1h-inden-1-one
반응식
O[CH:2]=[C:3]1[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]1=[O:12].C([O-])(=O)C.[NH4+].C[NH:19]C.CN.NC(O)C>C(O)C>[NH2:19][CH:2]=[C:3]1[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]1=[O:12]참가 물질
7
실험 절차
The 2-hydroxymethylene-1-indanone is then reacted with the appropriate nitrogen compound e.g. ammonium acetate, dimethyl amine, monomethyl amine or aminoethanol, in ethanol or any other suitable solvent to yield a 2-aminomethylene-1-indanone which is then dried and recrystallized from benzene or any other suitable solvent.
출처 및 근거
- ORD 기록
- ord-db4c2f4080974e02883bdad2a968ddeb
- 출처 데이터셋
- uspto-grants-1979_08
- 특허 번호
- US04164514
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