1-Butanol → n-Butylphosphorodichloridate

HRID 263846노트

반응식

HRID 263846 반응식
[P:1]([Cl:5])(Cl)([Cl:3])=[O:2].[CH2:6]([OH:10])[CH2:7][CH2:8][CH3:9]>C(Cl)(Cl)(Cl)Cl>[CH2:6]([O:10][P:1]([Cl:5])([Cl:3])=[O:2])[CH2:7][CH2:8][CH3:9]

참가 물질

4

반응물 2

HCID 2631-ButanolHCID 24813Phosphorus oxychloride

생성물 1

HCID 137039n-Butylphosphorodichloridate

시약·촉매·용매 1

HCID 5943Carbon Tetrachloride용매

실험 절차

The desired subtitled compound was prepared substantially in accordance with the procedure detailed in Example 8A, using 1.25 ml (13.5 mmol) of phosphorous oxychloride, 1 g (13.5 mmol) of butanol in 5 ml of carbon tetrachloride to provide a colorless oil.

후처리

  1. customto provide a colorless oil

출처 및 근거

ORD 기록
ord-c23a89090afc49b7acec677166ba8df0
출처 데이터셋
uspto-grants-1997_07
특허 번호
US05646111

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