Cytidine → HCID 22874746, 화합물

HRID 264741

반응식

HRID 264741 반응식
[C@@H:1]1([N:10]2[CH:17]=[CH:16][C:14]([NH2:15])=[N:13][C:11]2=[O:12])[O:9][C@H:6]([CH2:7][OH:8])[C@@H:4]([OH:5])[C@H:2]1[OH:3].[H-].[Na+].Br[CH2:21][CH2:22][CH3:23]>CN(C=O)C>[CH2:21]([O:3][C@@H:2]1[C@H:4]([OH:5])[C@@H:6]([CH2:7][OH:8])[O:9][C@H:1]1[N:10]1[CH:17]=[CH:16][C:14]([NH2:15])=[N:13][C:11]1=[O:12])[CH2:22][CH3:23]

참가 물질

5

반응물 3

HCID 6175CytidineHCID 78401-BromopropaneHCID 24758Sodium hydride

생성물 1

HCID 22874746HCID 22874746, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

Cytidine (16.5 g, 0.068 mol) was treated with sodium hydride (4.5 g) and bromopropane (15 ml) in DMF (150 ml) at room temperature for three days. The resulting reaction mixture was used directly in the next step (see Example 83).

후처리

  1. customThe resulting reaction mixture

출처 및 근거

ORD 기록
ord-ebe1e5446f864986a5d6bd5adfda59ed
출처 데이터셋
uspto-grants-1997_07
특허 번호
US05646265

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