Hydrazine hydrate (1:1) → 2-Amino-2'-chloro-5-nitrobenzophenone hydrazone

HRID 267400노트

반응식

HRID 267400 반응식
[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12])=O.O.[NH2:21][NH2:22]>C(O)COCCO>[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][C:3]=1[C:4](=[N:21][NH2:22])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12]

참가 물질

4

반응물 2

HCID 24654Hydrazine hydrate (1:1)HCID 748302-Amino-5-nitro-2'-chlorobenzophenone

생성물 1

HCID 867330932-Amino-2'-chloro-5-nitrobenzophenone hydrazone

시약·촉매·용매 1

HCID 8117Diethylene Glycol용매

실험 절차

In the manner given in Preparation 1, 2-amino-2'-chloro-5-nitrobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 2-amino-2'-chloro-5-nitrobenzophenone hydrazone.

출처 및 근거

ORD 기록
ord-7f8dae1f59424057b1fe72dcaeac3514
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03941803

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